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通过对中、上鞍山群变质沉积岩中黑云母化学成分的对比,确认区内两层位黑云母化学组分存在一定差异,这种差异主要反映了其形成时变质条件的不同。随变质程度增加,区内黑云母的Si、AI~Ⅵ,Fe~(3 )、Mg和K含量增加,而Fe~(2 )、Al~Ⅳ和CH降低,Mg/Fe~(2 )比值从1.00增至2.18。中鞍山群黑云母变质温度为550—620℃,变质压力在5×10~8Pa左右;上鞍山群黑云母变质温度为450-500℃,变质压力低于5×10~8Pa。黑云母含铁系数(f)可作为鞍山地区寻找富铁矿的一种标志。 相似文献
74.
The ability of several ab initio models to predict experimental 29Si-NMR chemical shift is examined. The shielding values of trimethylsilyl chloride (A), t-butyldimethylsilyl chloride (B)
and allytrimethylsilane (C) are calculated by GIAO, CSGT and IGAIM methods, using HF/6–31G*, B3LYP/6-31G*, HF/6–311+G**, B3LYP/6–311+G** and MPW1PW91/6–311+G** models respectively. The 29Si chemical shifts calculated by GIAO method using HF/6–311+G** model are highly in agreement with those obtained experimentally. All of the models above reproduce the trends of chemical
shifts in all cases studied, suggesting that the models are of practical value. 相似文献
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A peat bed found under solifluction deposits on Godøya island, western Norway, accumulated during a few decades around 11 000 yr BP, at the end of the Allerød period of the Late Weichselian. Palaeoecological investigations showed a local vegetation succession on wet sand culminating in a mire community dominated by Carex nigra. Periodic flooding brought in sand and silt, which decreased as drainage was impeded sufficiently for standing water to develop. The surrounding terrestrial vegetation was dominated by Salix scrub, with some open heath and alpine habitats nearby. Apart from two aquatic species, the 29 insect taxa recorded are characteristic of alpine heaths, plant litter (under Salix scrub) and stream-sides. Their remains, together with the terrestrial plant macrofossils, were washed into the mire from nearby. Because the fossils are locally derived, the environmental reconstructions are of the actual conditions at Godøy at ca. 11 000 yr BP. Palaeotemperature estimates from beetles and plants are in agreement. The coleopteran estimates (Mutual Climatic Range Method) suggest mean July temperatures of 10–13°C, slightly cooler than today (13.5°), and January temperatures between +1 and ?10°C, similar to or much colder than today. Summer temperature estimates from individual plant taxa indicate that temperatures during the Allerød period were similar to today's, but estimates from the reconstructed vegetation and timber-line positions give estimates up to 3.5° cooler. Temperatures fell 2.5–7.5°C at the Younger Dryas. This abrupt and severe cooling initiated the solifluction processes on Godøya that buried the peat. The Godøy peat bed and its contained fossils provide a rare glimpse of Allerød biota and environments at the local (site) scale. 相似文献
77.
以五氧化二钒为熔剂,用热解分离富集痕量溴,吸收于0.036mol/l 氢氧化钾中,在1.34mol/l 硫酸和硝酸混合溶液中,溴离子催化高锰酸钾对碘的氧化,用苯萃取未反应碘,然后用硫氢酸汞—硫酸高铁铵比色法测定溴。本方法灵敏度高,远择性好,操作简便、快速,方法检出限为0.35ppm 溴,标准偏差为11.63%。 相似文献
78.
作者根据庐山羊角岭红色泥砾的岩性特征,从地形和堆积物的宏观和微观特征进行分析研究,得出庐山有第四纪冰川。 相似文献
79.
W. N. Mussel E. Murad J. D. Fabris W. S. Moreira J. B. S. Barbosa C. C. Murta W. P. Abrahão J. W. V. De Mello V. K. Garg 《Physics and Chemistry of Minerals》2007,34(6):383-387
We studied a chalcopyrite from a Cu ore deposit in Rio Grande do Sul, Brazil, by Mössbauer spectroscopy at room temperature and 110 K. Supporting methods to check for sample purity and to characterize further sample properties were slow-scanning X-ray powder diffraction and optical and microprobe analyses of polished sections of selected grains. Chemical analyses obtained using a scanning electron microscope equipped with an energy-dispersive X-ray spectrometer showed the sample to consist of homogeneous and essentially stoichiometric chalcopyrite (CuFeS2). Mössbauer spectra taken at both the above temperatures consist of asymmetric magnetically ordered patterns with unequal intensities of the line pairs 1–6 and 2–5, pointing to the existence of non-equivalent or multiple Fe sites. Least-squares fittings evidenced that the resonance intensity ratio of subspectrum with lower quadrupole shift (indicative of a more symmetric environment) to that with higher shift is 69:31, at room temperature, and 68:32, at 110 K. Rietveld refinement of the XRD data indicates the existence of tetragonal [a = 0.52855(1) and c = 1.0412(1) nm] and cubic [a 0 = 0.5273(2) nm] modifications in a proportion of 74:26, in good agreement with the Mössbauer data. The saturation magnetization of the sample was 32.7 J/(T kg), confirming the oxidation state of Fe as trivalent and pointing to little to no spin canting. 相似文献
80.
北京地区铬的土壤化学地理 总被引:7,自引:0,他引:7
本文以化学地理学的观点,讨论了铬在土壤中的来源,分布规律,迁移和残留累积,生态和环境效应,循环与平衡,预测和评价。 相似文献